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Talk:MDMA Synthesis: Difference between revisions
>White Grammatics |
>Indigo Added some more information, nothing crazy just a bit of checking up and adding some more as I had a bit of free time |
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{{Proofread}} | |||
{{SubstanceBox/MDMA}} | {{SubstanceBox/MDMA}} | ||
{{Disclaimer}} | {{Disclaimer}} | ||
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*Ph Pen | *Ph Pen | ||
*Ax | *Ax | ||
*Shovel | |||
*Sharp Knife | *Sharp Knife | ||
*Colander | *Colander | ||
*1qt Steel Pot | *1qt Steel Pot | ||
*Funnel | *Separatory Funnel | ||
*Turkey Baster | *Turkey Baster | ||
*3 Extention Clamps | *3 Extention Clamps | ||
*Clamp Fastener | *Clamp Fastener | ||
*Dry Pan | |||
*Cheesecloth | |||
==Chemicals and Reagants== | ==Chemicals and Reagants== | ||
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*5l Everclear | *5l Everclear | ||
*10ml Magnesium Sulphate | *10ml Magnesium Sulphate | ||
*31.45% Muriatic Acid HCL | *31.45% Muriatic Acid HCL | ||
*100% NaOH | *100% NaOH | ||
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*500g Paraformaldehyde | *500g Paraformaldehyde | ||
*Peanut Oil | *Peanut Oil | ||
*500ml Xylene | *500ml Xylene | ||
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#Grease the connections between the adaptor and the Condenser, then connect and twist. Secure condenser with clamp and stand. | #Grease the connections between the adaptor and the Condenser, then connect and twist. Secure condenser with clamp and stand. | ||
Diagram of | Diagram of the condenser being connected: | ||
[[Media:CondencerDistill.jpeg]] | [[Media:CondencerDistill.jpeg]] | ||
#Grease and connect the Vaccum adapter, then the 250ml Round Bottom Flask. | #Grease and connect the Vaccum adapter, then the 250ml Round Bottom Flask. | ||
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#Now you know how to put the Pieces together, you will need to occasionally add and remove or swap parts out, this will be explained further as we go along. | #Now you know how to put the Pieces together, you will need to occasionally add and remove or swap parts out, this will be explained further as we go along. | ||
===Preparation=== | ===Preparation=== | ||
#Before starting I recommend cleaning everything with Tide detergent and warm water, making sure you have | #The reason the Ax and shovel are listed is so that you can dig and cut your own segments of sassafrass root. This synth requires a good deal of sassafrass root, so start by collecting a lot of roots and then skin the bark with the sharp knife. | ||
# | #Place the shredded bark into mason jars and save it for later | ||
#Before starting I recommend cleaning everything with Tide detergent and warm water, making sure you have PLENTY of time to complete. A weekend should be ideal. | |||
===Extraction of Sassafrass Oil=== | |||
#Start by placing all of your shredded bark into a colander over a quart steel pot, run water over the bark sifting it to wash it, then let it sit and dry completely. DRYING CAN TAKE WEEKS | |||
#Empty and clean the 1 qt pot, place the shredded bark inside and fill with water just above the bark. Cook at 25C for 6+ hours. | |||
''This step is a little, well, ''cheap'' but It's a lot easier than some other more advanced methods so I feel it would be best suited for this Synth as it's oriented towards people that have never touched so much as a flask in their lives.'' | |||
# | |||
===Distillation for MethylAmine.HCl=== | |||
#As always, clean all equipment and make sure you have plenty of time available | |||
#Set up your Distilling Apparatus '''WITHOUT''' the Vacuum Aspirator, This is just a simple distillation, if you need help I recommend reading "''The Organic Chem Lab Survival Manual''" By Zubrick, It's listed as the third reference on this page. | |||
# | |||
[[User:Indigo|Indigo]] ([[User talk:Indigo|talk]]) | [[User:Indigo|Indigo]] ([[User talk:Indigo|talk]]) | ||
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#https://erowid.org/archive/rhodium/chemistry/brightstar.mdma.html | #https://erowid.org/archive/rhodium/chemistry/brightstar.mdma.html | ||
#https://www.leaf.tv/articles/how-to-extract-sassafras-oil/ | #https://www.leaf.tv/articles/how-to-extract-sassafras-oil/ | ||
#https://archive.org/stream/TheOrganicChemLabSurvivalManual/TheOrganicChemLabSurvivalManual-Zubrick#page/n0/mode/2up | |||