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| {{SubstanceBox/MDMA}}
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| {{Disclaimer}}
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| This synth requires a basic understanding of Organic Chemistry (Instructions include How-To use the lab equipment required) and access to a few somewhat difficult to obtain materials. This synth makes 15g of pure MDMA Crystals.
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| ==Lab Equipment==
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| *24/40 500mL Round Bottom Flask, Ground Glass Joints
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| *24/40 1000mL Round Bottom Flask, Ground Glass Joints
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| *24/40 250mL Round Bottom Flask, Ground Glass Joints
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| *24/40 Condenser, Ground Glass Joints
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| *24/40 Distillation Adapter, Ground Glass Joints
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| *24/40 Vacuum Adapter, Ground Glass Joints
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| *24/40 Thermometer Adapter, Ground Glass Joints
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| *0-300C Laboratory Thermometer
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| *24/40 3-Way Adapter
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| *3 Ten Inch Chemistry Stands
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| *Digital Hotplate/Magnetic Stirrer
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| *Teflon Coated Magnetic Stir Bar
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| *Glass Water Aspirator
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| *Boiling Stones
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| *10 ft Vaccum Tubing
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| *Vaseline
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| *Pyrex 100ml Beaker
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| *10 Quart Mason Jars
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| *Three Beam Analytical Balance
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| *Ph Pen
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| *Ax
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| *Sharp Knife
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| *Colander
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| *1qt Steel Pot
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| *Funnel
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| *Cheesecloth
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| *Turkey Baster
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| *3 Extention Clamps
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| *Clamp Fastener
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| ==Chemicals and Reagants==
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| '''Buy more than listed, that way mistakes can be easily fixed!'''
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| ''Some measurements listed here are slightly overshot for this very reason''
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| *Tide Detergent
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| *Lots of Water (Boiled)
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| *Lots of Sassafras Root Bark(See Preparation)
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| *350ml Dimethylformamide
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| *120g p-Benzoquinone
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| *2g Palladium Chloride
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| *5oom Methylene Chloride
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| *1g HgCl2 Salt
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| *5l Everclear
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| *10ml Magnesium Sulphate
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| *Dry Pan
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| *31.45% Muriatic Acid HCL
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| *100% NaOH
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| *500g Ammonium Chloride
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| *500g Paraformaldehyde
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| *Peanut Oil
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| *500ml
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| *500ml Xylene
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| ==Synth==
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| ===Lab Setup===
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| #First off, make sure your lab has access to running water for the aspirator to make use of, water runs through it to create a vacuum inside of the distillation apparatus.
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| #Start by arranging your stands beside one another, then Place your clamps at a decent height, enough for an oil bath to fit under your flask.
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| #Clamp your 500ml Round Bottom Flask to the left stand around the neck of the Flask.
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| #Grease the tops of the joints of the Flask and the 3-way adapter and connect. then twist.
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| How to grease joints:
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| [[Media:DistillGrease.jpeg]]
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| Diagram of 3-way adapter being connected:
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| [[Media:3WayAdapterDistill.jpeg]]
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| #Grease the connections between the adaptor and the Condenser, then connect and twist. Secure condenser with clamp and stand.
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| Diagram of condencer being connected:
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| [[Media:CondencerDistill.jpeg]]
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| #Grease and connect the Vaccum adapter, then the 250ml Round Bottom Flask.
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| #Ensure everything is tight and add clamps to ensure nothing moves.
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| What your setup should look like:
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| [[Media:VaccumDistill.jpeg]]
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| #Now you know how to put the Pieces together, you will need to occasionally add and remove or swap parts out, this will be explained further as we go along.
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| ===Preparation===
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| #Before starting I recommend cleaning everything with Tide detergent and warm water, making sure you have pre-measured everything, and make sure you have PLENTY of time to complete. A weekend should be ideal.
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| #WORK IN PROGRESS, more steps will be added later this week, taking a break for the time being. :))
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| [[User:Indigo|Indigo]] ([[User talk:Indigo|talk]])
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| ==See also==
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| *[[MDMA]]
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| *[[Experience index#MDMA|MDMA Trip Reports]]
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| ====References====
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| <references />
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| #https://erowid.org/archive/rhodium/chemistry/brightstar.mdma.html
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| #https://www.leaf.tv/articles/how-to-extract-sassafras-oil/
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