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MDMA/Synthesis: Difference between revisions
>David Hedlund |
>David Hedlund === External links === * [https://isomerdesign.com/PiHKAL/read.php?domain=pk&id=109 MDMA (PiHKAL: A Chemical Love Story)] |
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Two hundred milligrams of MDMA HCl was dissolved in 2 ml of buffer. Two different buffers, phosphate buffer, pH 7, and carbonate buffer, pH 10, were tested. The suspension was vigorously shaken (25 min) following by the addition of 200 ml of ''n''-heptane, containing diphenylamine as an internal standard, and then again shaken (25 min). The extracts were subjected to GC/MS analysis, and impurity profiles were obtained. | Two hundred milligrams of MDMA HCl was dissolved in 2 ml of buffer. Two different buffers, phosphate buffer, pH 7, and carbonate buffer, pH 10, were tested. The suspension was vigorously shaken (25 min) following by the addition of 200 ml of ''n''-heptane, containing diphenylamine as an internal standard, and then again shaken (25 min). The extracts were subjected to GC/MS analysis, and impurity profiles were obtained. | ||
=== External links === | |||
* [https://isomerdesign.com/PiHKAL/read.php?domain=pk&id=109 MDMA (PiHKAL: A Chemical Love Story)] | |||
<references/> | <references/> | ||
[[category:Chemical synthesis]] | [[category:Chemical synthesis]] | ||