Talk:MDMA Synthesis: Difference between revisions

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+{{headerpanel|{{Disclaimer}}}}
+{{SubstanceBox/MDMA}}
+This synth requires a basic understanding of Organic Chemistry (Instructions include How-To use the lab equipment required) and access to a few somewhat difficult to obtain materials. This synth makes 15g of pure MDMA Crystals.
+==Lab Equipment==
+*24/40 500mL Round Bottom Flask, Ground Glass Joints
+*24/40 1000mL Round Bottom Flask, Ground Glass Joints
+*24/40 250mL Round Bottom Flask, Ground Glass Joints
+*24/40 Condenser, Ground Glass Joints
+*24/40 Distillation Adapter, Ground Glass Joints
+*24/40 Vacuum Adapter, Ground Glass Joints
+*24/40 Thermometer Adapter, Ground Glass Joints
+*0-300C Laboratory Thermometer
+*24/40 3-Way Adapter
+*3 Ten Inch Chemistry Stands
+*Digital Hotplate/Magnetic Stirrer
+*Teflon Coated Magnetic Stir Bar
+*Glass Water Aspirator
+*Boiling Stones
+*10 ft Vaccum Tubing
+*Vaseline
+*Pyrex 100ml Beaker
+*10 Quart Mason Jars
+*Three Beam Analytical Balance
+*Ph Pen
+*Ax
+*Shovel
+*Sharp Knife
+*Colander
+*1qt Steel Pot
+*Separatory Funnel
+*Turkey Baster
+*3 Extention Clamps
+*Clamp Fastener
+*Dry Pan
+*Cheesecloth
+==Chemicals and Reagants==
+'''Buy more than listed, that way mistakes can be easily fixed!'''
+''Some measurements listed here are slightly overshot for this very reason''
+*Tide Detergent
+*Lots of Water (Boiled)
+*Lots of Sassafras Root Bark(See Preparation)
+*350ml Dimethylformamide
+*120g p-Benzoquinone
+*2g Palladium Chloride
+*5oom Methylene Chloride
+*1g HgCl2 Salt
+*5l Everclear
+*10ml Magnesium Sulphate
+*31.45% Muriatic Acid HCL
+*100% NaOH
+*500g Ammonium Chloride
+*500g Paraformaldehyde
+*Peanut Oil
+*500ml Xylene
+==Synth==
+===Lab Setup===
+#First off, make sure your lab has access to running water for the aspirator to make use of, water runs through it to create a vacuum inside of the distillation apparatus.
+#Start by arranging your stands beside one another, then Place your clamps at a decent height, enough for an oil bath to fit under your flask.
+#Clamp your 500ml Round Bottom Flask to the left stand around the neck of the Flask.
+#Grease the tops of the joints of the Flask and the 3-way adapter and connect. then twist.
+How to grease joints:
+[[Media:DistillGrease.jpeg]]
+Diagram of 3-way adapter being connected:
+[[Media:3WayAdapterDistill.jpeg]]
+#Grease the connections between the adaptor and the Condenser, then connect and twist. Secure condenser with clamp and stand.
+Diagram of the condenser being connected:
+[[Media:CondencerDistill.jpeg]]
+#Grease and connect the Vaccum adapter, then the 250ml Round Bottom Flask.
+#Ensure everything is tight and add clamps to ensure nothing moves.
+What your setup should look like:
+[[Media:VaccumDistill.jpeg]]
+#Now you know how to put the Pieces together, you will need to occasionally add and remove or swap parts out, this will be explained further as we go along.
+===Preparation===
+#The reason the Ax and shovel are listed is so that you can dig and cut your own segments of sassafrass root. This synth requires a good deal of sassafrass root, so start by collecting a lot of roots and then skin the bark with the sharp knife.
+#Place the shredded bark into mason jars and save it for later
+#Before starting I recommend cleaning everything with Tide detergent and warm water, making sure you have  PLENTY of time to complete. A weekend should be ideal.
+===Extraction of Sassafrass Oil===
+#Start by placing all of your shredded bark into a colander over a quart steel pot, run water over the bark sifting it to wash it, then let it sit and dry completely. DRYING CAN TAKE WEEKS
+#Empty and clean the 1 qt pot, place the shredded bark inside and fill with water just above the bark. Cook at 25C for 6+ hours.
+''This step is a little, well, ''cheap'' but It's a lot easier than some other more advanced methods so I feel it would be best suited for this Synth as it's oriented towards people that have never touched so much as a flask in their lives.''
+#
+===Distillation for MethylAmine.HCl===
+#As always, clean all equipment and make sure you have plenty of time available
+#Set up your Distilling Apparatus '''WITHOUT''' the Vacuum Aspirator, This is just a simple distillation, if you need help I recommend reading "''The Organic Chem Lab Survival Manual''" By Zubrick, It's listed as the third reference on this page.
+#
+[[User:Indigo|Indigo]] ([[User talk:Indigo|talk]])
+==See also==
+*[[MDMA]]
+*[[Experience index#MDMA|MDMA Trip Reports]]
+==References==
+<references />
+#https://erowid.org/archive/rhodium/chemistry/brightstar.mdma.html
+#https://www.leaf.tv/articles/how-to-extract-sassafras-oil/
+#https://archive.org/stream/TheOrganicChemLabSurvivalManual/TheOrganicChemLabSurvivalManual-Zubrick#page/n0/mode/2up